課程資訊
課程名稱
分析化學特論一
SPECIAL TOPICS IN ANALYTICAL CHEMISTRY(Ⅰ) 
開課學期
94-2 
授課對象
理學院  化學系  
授課教師
張哲政 
課號
Chem5031 
課程識別碼
223 U1110 
班次
 
學分
全/半年
半年 
必/選修
選修 
上課時間
星期二2(9:10~10:00)星期四3,4(10:20~12:10) 
上課地點
化121教室 
備註
外系所學生選修需經授課教師同意
限學士班三年級以上
總人數上限:50人 
 
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課程概述

分析化學特論一

Instructor:

Prof. Che-Chen Chang

Office:

Room 203, Isotope Building

Email:

cchang@ntu.edu.tw

Course Description:

Overview: An introduction to the basic theory and practice underlying important electroanalytical methods and electron spectroscopy as well as their applications

Prerequisites:

Analytical Chemistry (I),Analytical Chemistry (II),or equivalents

Lecture schedule:
Tue., 9:10 AM - 10:00 AM,Fri., 10:20 AM -12:10 PM

Credit hours: 3

Course Content:

This course is presented in a lecture/discussion format. The content of the course includes Ion conductance, ion mobility, electrical conductivity, transport numbers, electrical double layer, activity coefficient of electrolytes - ionic strength, Debye Huckel law, thermodynamics of electrochemical cells, galvanic couple, electrode process, liquid junction potential, overvoltage, anodic dissolution of metals, ion selective electrodes, redox titration, electrochemical instrumentation, electrolysis, potential measurement, amperometric sensor, coulometric measurement, polarographic measurement, voltammetric measurement, electronic structure, jellium model, density of states, Fermi energy, band structure, thermionic emission, photoelectron emission, field emission, beam-specimen interaction, surface ionization, resonance neutralization, resonance ionization, surface penning ionization, spectroscopic instrumentation, transmission electron microscopy, scanning electron microscopy, electron probe microanalysis, photoelectron spectroscopy, Auger spectroscopy, scanning Auger microscopy, electron energy loss spectroscopy

Testing:

The exams are primarily problems and short essays, not true-false or multiple choice. They will emphasize the course objectives of understanding the fundamental theory and concepts, operation principles, design, applications, strengths, and limitations of the electroanalytical and electron methods introduced. The content of the tests include the materials discussed in your textbook as well as those taught in the class. The final test is a comprehensive exam and will require you to integrate the class material in a meaningful way. Calculators used in the exam cannot contain any dictionary or graphic function.

Evaluation:

Grades for the course will be based upon the following schedule.

First Exam 30%

Second Exam 30%

Final Exam 40%

Total 100%

Make-up policy:

Make-up exams will not be permitted to those who miss the midterms or the final. Students should present records of clinic visits for missing the exam due to illness.

Class attendance:

Good, participatory attendance is essential to successful mastery of course material. Although the attendance will not be monitored daily, it is suggested that you do not take this course if you cannot come to the class or do not like to take notes.

Honor Code:

The NTU policies on cheating will be enforced.
 

課程目標
Course Objectives

This course provides students with an in-depth understanding about the background theory and operation principles of different analytical methods that employ electrons. The specific objectives of the course are to help students

- to become familiar with the various electroanalytical and electron beam/spectroscopic methods currently available

- to develop an understanding of the theories upon which the principles of the electroanalytical and electron beam/spectroscopic procedures are based

- to understand the correlations of chemical analysis concepts and of various controllable and measurable (potential, current, coulometric, voltametric) quantities

- to learn how different analytical methods that employ electrons are used to analyze samples

- to understand the basic strengths and limitations of each electroanalytical and electron beam/spectroscopic method

- to learn to apply chemical equilibria, stoichiometry, thermodynamics and kinetics to solve analytical problems using electroanalytical and electron beam/spectroscopic methods
 
課程要求
 
預期每週課後學習時數
 
Office Hours
 
指定閱讀
 
參考書目
Text:

Daniel C. Harris, Quantitative Chemical Analysis (6th Edition), W.H. Freeman and Company

Douglas A. Skoog, F. James Holler, Timothy A. Nieman,, Principles of Instrumental Analysis (5th Edition)
 
評量方式
(僅供參考)
 
No.
項目
百分比
說明
1. 
First Exam 
30% 
 
2. 
Second Exam 
30% 
 
3. 
Final Exam 
40% 
 
 
課程進度
週次
日期
單元主題